By leveraging the inherent low temperature design for this used as a SPD I run mantle temperatures typically up to 100°C lower than a vertical more traditional SPD which affords a tremendous advantage when it comes to fraction rejection rates between fractions. These are very low temps to see...
Hard to say what other folks call affordable or not. My rig operates atop an Amish built buffet table. The cryogenic sublimation apparatus costs between $400-$500 dollars depending on where you get it. The vacuum pump must be able to pull a vacuum down to mean free path conditions (MFP) to...
D9 THC isolate just minutes out of deep vacuum where it was refined to this purity. Shown is the cold finger of a cryogenic sublimation apparatus. Final pass through this apparatus took place at 127° C and ¾ of one micron nominal. THC is subject to oxidation into CBN and so time outside a vacuum...
I put a site up for my photos and stuff now for the technically interested. I will put this sort of thing up there because then I can post high quality vids too. http://beakercracked.com/
I get my concentrate from an ommp grower through my ommp care provider almost always. I am free to purchase from dispensaries as well but that is not how I normally would get the concentrate. I honestly do not know how they concentrate the oil out of the plant.
I start with crude normally that...
Thanks! Check out this shot of the stuff this morning. I love this hobby because the cool pictures plus.... if you say nice things to me it just encourages dude so you get a picture I just snapped. Truthfully this stuff is likely a bit more potent than most would care for. I can tell a guest to...
I rarely measure for yield except a few times. When the concentrate tests at 60% THC or so I can get 57% of total weight returned as this kind of isolate when I was careful and measured. The problem with measuring is that a lot of the compound transfers from run to run meaning that I don’t...
Cryogenic sublimator shown above during high purity run. I propose to use this vessel. That is Delta 9 THC isolate shown dripping and collecting as a bodacious layer on the cold finger.
I believe I have a way to verifiably determine the exact boiling point of THC in my own lab in a way that I...
Started as brown crude. Dewax over alumina. Then vacuum distillation to remove terps only. Then DCVC to remove generally purple colored compounds always present as a trace and which will age into darker purple and show up later. Then two passes through my cryogenic sublimator under mean free...