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D9 THC isolate just minutes out of deep vacuum where it was refined to this purity. Shown is the cold finger of a cryogenic sublimation apparatus. Final pass through this apparatus took place at 127° C and ¾ of one micron nominal. THC is subject to oxidation into CBN and so time outside a vacuum...

http://beakercracked.com/blog/micro-thc-refinement

This is a blog post with video showing how steam disitllation works to help purify crude. http://beakercracked.com/blog/steam-distillation-of-extract

Here are the harvest photos from the video link. It came out great.

Cryogenic sublimator shown above during high purity run. I propose to use this vessel. That is Delta 9 THC isolate shown dripping and collecting as a bodacious layer on the cold finger. I believe I have a way to verifiably determine the exact boiling point of THC in my own lab in a way that I...

The compound collecting on the cold finger is D9 THC isolate. The red LED indicates the heating mantle temp in Celsius. Pressure reads ¾ of one micron. Room pressure is normally 760,000 microns. The sensor for the heating mantle is under the glass and between the heating mantle. The oil temp is...

These are the highlights of the steps I took this month to turn crude concentrate medicine provided me into Delta 9 THC isolate. The techniques vary from month to month but generally follow this progression. This step is an overnight soak in rubbing alcohol of the crude concentrate. The RA is...

Horizontal configuration shown with terpene fraction collecting in first collection bulb. Bulb will be swapped out for a clean one to collect cannabinoids. Boiling flask contains rosin pressed concentrate crude. Time lapse of cannabinoid fraction coming over...

This is fresh off the cold finger out of deep vacuum. When exposed to air it turns red pretty fast so it is stored in a vacuum chamber. Starting compound was dark crude. This is high refinement and is a purity approaching absolute.

It vapes like velvet.

After multiple steps to obtain high purity THC the product is stirred completely. It is very thick but liquid. When a vacuum is pulled it gives a chance then to purge trace gases/volitiles as the entrapped air expands and increases the surface area exponentially. The oil swells to many times its...

Shot of cryogenic sublimator, temperature set point at mantle, and vacuum reading. This is this months med and my aches and pains are anxious for this run to finish up. Starting dispensary extract was deep brown, almost dark and smelled terpy but nice. There are steps before this shot but I like...

Let me pass on a tip for those wanting to "clean up" their extract. It is just another way to help purify and is generally based of a technique that I have learned to call counter current seperation. It is an old idea. I have stopped videos so I will describe it. This is a long post that...

This is nearly pure D9 THC fresh out of the sublimation apparatus. This is the same pure D9 THC compound from above but a day or two later when left out. This is third run D9 THC as in the top photo but with waxes left in. Here is that same dab today but a few weeks later and being dipped...

Here is a copy paste from Oregon Statute that tries to define for us what is and what is not legal. I look up from time to time the law so I understand it and keep legal. HOWEVER....something jumped out at me after vaping my morning bag of highly refined oil. This is a fun thing but I have to...

Youtube began pulling videos I made about marijuanna refinement saying they violated community standards. All my videos have now been deleted and I will not be posting any more. Sorry. As far as I know all my activities are legal in Oregon but it violates Youtube policy.

This is a cryogenic sublimation apparatuse being used to further refine extract towards purities approaching absolute. The measured pressue by Pirani style sensor in the system at this moment of the picture was recorded at ¾ of one micron. Temperture at the boiling puddle is approximately 140C...