Lipids and waxes not solidifying

  • Thread starter Just me66
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J

Just me66

5
3
Hello
So after 6 years of vaping shatter I decided to do a winterization of 11 grams of Pineapple Express hard shatter.
I used 10 mls of 190 everclear per gram of shatter. Mixed well and placed in the freezer. Which the temp is about 14 degrees. I left in the freezer for about 27 hrs. I could see the lipids and such in the mix. But, it wasn’t solids at all. It looked like it was milky.
I strained in the freezer. I found only a tiny bit of lipids on the un bleached coffee filter. I placed the mix on a reptile heat mat that ran at 88 degrees ish. The everclear evaporated and I could see what was that milky stuff in my shatter. But some of the shatter goo was clear as can be. So I didn’t vac purge. Can anyone please tell me what I did wrong? I’m thinking maybe not enough freezer time?
Should I redo and leave in the freezer for 48 hrs or til the lipids solidify? Dry ice is hard to get in the country.
In the pic you can see all the white.

I did reclaim in 91 iso and it would whiten up when evaporating but go away after it dried.
 
Lipids and waxes not solidifying
J

Just me66

5
3
The pic is the everclear mix and not reclaim. But I think you can tell.
 
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